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The solid-phase method was conceived and elaborated by R. B Merrifield ( 10 ). The concept of SPPS ( Fig. 1 ) is to retam chemtstry proven m solution and to add a covalent attachment step that links the nascent peptide chain to an msoluble polymeric support.
Merrifield RB (1963) Solid-phase peptide synthesis. synthesis of a tetrapeptide. J Am Chem Soc 85:2149–2154 Merrifield RB (1985) Solid-phase peptide synthesis (nobel lecture). Science 232:341–347 Bergmann M, Zervas L (1932) Über ein allgemeines verfahren der peptid-synthese. Berichte 65:1192–1201
Divergent synthesis. In chemistry a divergent synthesis is a strategy with the aim to improve the efficiency of chemical synthesis. It is often an alternative to convergent synthesis or linear synthesis. In one strategy divergent synthesis aims to generate a library of chemical compounds by first reacting a molecule with a set of reactants.
液相合成. 液相多肽合成（Liquid-phase peptide synthesis）是一種多肽合成的經典方法。雖然現在大多數在實驗室中已經被固相多肽合成（見下文）所取代，但液相多肽合成仍有在工業上大規模生產多肽的可用性。
Synthesis 2020, 52, A–U Georg Thieme Verlag KG, Rüdigerstraße 14, 70469 Stuttgart, Germany Imprimatur: Date, Signature ss-2020-c0384-st.fm 9/23/20 Synthesis S. R. Manne et al. Special Topic OxymaPure Coupling Reagents: Beyond Solid-Phase Peptide Synthesis Srinivasa Rao Mannea Beatriz G. de la Torrea,b Ayman El-Faham*c,d Fernando Albericio*a ...
Carbonsäurebromide werden insbesondere als Reagenzien in der organischen Synthese eingesetzt, siehe Abschnitt Reaktionen. Bei der Acetylbromid-Methode wird Pflanzenmaterial mit Acetylbromid in Essigsäure umgesetzt und enthaltenes Lignin im Sauren in Lösung gebracht, sodass es photometrisch quantitativ bestimmt werden kann.
27. Mai 2022 · This review summarizes the solid- and solution-phase syntheses of α-peptides and specialty peptides, including N-methylated peptides, β-peptides, and cyclic peptides, reported mainly after 2017. The recently reported mesoflow peptide syntheses (inner diameter of the reaction channels > 1 mm), the microflow automated syntheses, and in-line analysis are covered in this review.
